TY - JOUR
T1 - Y2O3 nanoparticle reinforced H13 tool steel fabricated via electron beam melting
T2 - Variant selection, microstructural evolution, and strengthening mechanisms
AU - Deng, Jiaqi
AU - Wang, Gengjie
AU - Qi, Hongjun
AU - Ma, Hanyu
AU - Jian, Yongxin
AU - Huang, Zhifu
N1 - Publisher Copyright:
© 2025 Elsevier B.V.
PY - 2026/1
Y1 - 2026/1
N2 - H13 tool steel is widely applied in the die industry owing to its excellent thermal strength and wear resistance. However, components fabricated via electron beam melting (EBM) still suffer from unsatisfactory strength–ductility balance. In this study, yttrium oxide (Y2O3)/H13 composites were fabricated using EBM with 0.2 wt% Y2O3 nanoparticles added to optimize the microstructure and mechanical performance. The results showed that Y2O3 nanoparticles suppressed prior austenite grain (PAG) coarsening and promoted heterogeneous nucleation, resulting in finer and more equiaxed grains. The composite microstructure changed from an interwoven martensite–bainite structure to a continuous martensitic matrix with discrete bainitic islands, accompanied by higher martensite content. Furthermore, the refinement of PAGs improved variant selection, increasing the proportion of high-angle grain boundaries and improving crack resistance. Consequently, the Y2O3/H13 composite exhibited a yield strength of 1463 MPa, an ultimate tensile strength of 1927 MPa, and a total elongation of 11.8 %, outperforming EBM-fabricated H13 steel in both strength and ductility. Quantitative analysis revealed that the strength improvements primarily resulted from grain refinement strengthening provided by finer grains, dislocation strengthening associated with the high dislocation density, and dispersion strengthening introduced by the added Y2O3 nanoparticles. These findings emphasize the importance of ceramic particles in tailoring microstructure to overcome the strength–ductility tradeoff, providing a promising avenue for the development of high-performance advanced tool steel.
AB - H13 tool steel is widely applied in the die industry owing to its excellent thermal strength and wear resistance. However, components fabricated via electron beam melting (EBM) still suffer from unsatisfactory strength–ductility balance. In this study, yttrium oxide (Y2O3)/H13 composites were fabricated using EBM with 0.2 wt% Y2O3 nanoparticles added to optimize the microstructure and mechanical performance. The results showed that Y2O3 nanoparticles suppressed prior austenite grain (PAG) coarsening and promoted heterogeneous nucleation, resulting in finer and more equiaxed grains. The composite microstructure changed from an interwoven martensite–bainite structure to a continuous martensitic matrix with discrete bainitic islands, accompanied by higher martensite content. Furthermore, the refinement of PAGs improved variant selection, increasing the proportion of high-angle grain boundaries and improving crack resistance. Consequently, the Y2O3/H13 composite exhibited a yield strength of 1463 MPa, an ultimate tensile strength of 1927 MPa, and a total elongation of 11.8 %, outperforming EBM-fabricated H13 steel in both strength and ductility. Quantitative analysis revealed that the strength improvements primarily resulted from grain refinement strengthening provided by finer grains, dislocation strengthening associated with the high dislocation density, and dispersion strengthening introduced by the added Y2O3 nanoparticles. These findings emphasize the importance of ceramic particles in tailoring microstructure to overcome the strength–ductility tradeoff, providing a promising avenue for the development of high-performance advanced tool steel.
KW - Electron beam melting
KW - H13 tool steel
KW - Mechanical properties
KW - Strengthening mechanisms
KW - Variant selection
UR - https://www.scopus.com/pages/publications/105024320483
U2 - 10.1016/j.msea.2025.149600
DO - 10.1016/j.msea.2025.149600
M3 - 文章
AN - SCOPUS:105024320483
SN - 0921-5093
VL - 951
JO - Materials Science and Engineering: A
JF - Materials Science and Engineering: A
M1 - 149600
ER -