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Synthesis and characterization of polyimide/silica nanocomposite films

  • M. Y. Zhang
  • , S. J. Zeng
  • , T. Q. Dong
  • , Y. Fan
  • , Q. Q. Lei
  • Harbin University of Science and Technology

科研成果: 书/报告/会议事项章节会议稿件同行评审

2 引用 (Scopus)

摘要

In the paper, a kind of polyimide nanocomposite films was made by synthesizing polyimide/silica nano-particle matrix resin through the hydrolysis and poly-condensation of varies ratio of tetraethoxysilane (TEOS) and dimethyldiethoxysilane (DMES) in the solution of polyamic acid (PAA) solution dissolved in N, N-dimethylacetamide (DMAc), followed by rotating it on glass substrates and heating at high temperature. The 3-aminopropyltriethoxysilane (APrTEOS), which serves as a coupling agent, was chosen to enhance the compatibility between the polyimide (PI) and the silica (SiO2). The chemical structure of the films was characterized by FT-IR. The results of TGA proved that the thermal stability can be improved by well dispersion of inorganic components not more than 16wt%.

源语言英语
主期刊名2007 International Conference on Solid Dielectrics, ICSD
357-359
页数3
DOI
出版状态已出版 - 2007
已对外发布
活动2007 International Conference on Solid Dielectrics, ICSD - Winchester, 英国
期限: 8 7月 200713 7月 2007

出版系列

姓名2007 International Conference on Solid Dielectrics, ICSD

会议

会议2007 International Conference on Solid Dielectrics, ICSD
国家/地区英国
Winchester
时期8/07/0713/07/07

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