Metal-free nitro-carbocyclization of 1,6-enynes with tBuONO and TEMPO

Xin Hua Hao; Pin Gao; Xian Rong Song; Yi Feng Qiu; Dong Po Jin; Xue Yuan Liu; Yong Min Liang

doi:10.1039/c5cc00872g

Metal-free nitro-carbocyclization of 1,6-enynes with ^tBuONO and TEMPO

Xin Hua Hao
, Pin Gao
, Xian Rong Song
, Yi Feng Qiu
, Dong Po Jin
, Xue Yuan Liu
, Yong Min Liang

Lanzhou University

科研成果: 期刊稿件 › 文章 › 同行评审

81 引用（Scopus）

摘要

A novel and convenient metal-free nitration and cyclization of 1,6-enynes has been developed. Two C-C bonds and one C-N bond were constructed in one process in this reaction. This transformation is proven to have relatively good functional-group applicability and can be scaled up to gram quantities in satisfactory yields. According to the following experimental facts and related literature reports, a radical pathway was involved in this transformation.

源语言	英语
页（从-至）	6839-6842
页数	4
期刊	Chemical Communications
卷	51
期	31
DOI	https://doi.org/10.1039/c5cc00872g
出版状态	已出版 - 21 4月 2015
已对外发布	是

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abstract = "A novel and convenient metal-free nitration and cyclization of 1,6-enynes has been developed. Two C-C bonds and one C-N bond were constructed in one process in this reaction. This transformation is proven to have relatively good functional-group applicability and can be scaled up to gram quantities in satisfactory yields. According to the following experimental facts and related literature reports, a radical pathway was involved in this transformation.",

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T1 - Metal-free nitro-carbocyclization of 1,6-enynes with tBuONO and TEMPO

AU - Hao, Xin Hua

AU - Gao, Pin

AU - Song, Xian Rong

AU - Qiu, Yi Feng

AU - Jin, Dong Po

AU - Liu, Xue Yuan

AU - Liang, Yong Min

PY - 2015/4/21

Y1 - 2015/4/21

N2 - A novel and convenient metal-free nitration and cyclization of 1,6-enynes has been developed. Two C-C bonds and one C-N bond were constructed in one process in this reaction. This transformation is proven to have relatively good functional-group applicability and can be scaled up to gram quantities in satisfactory yields. According to the following experimental facts and related literature reports, a radical pathway was involved in this transformation.

AB - A novel and convenient metal-free nitration and cyclization of 1,6-enynes has been developed. Two C-C bonds and one C-N bond were constructed in one process in this reaction. This transformation is proven to have relatively good functional-group applicability and can be scaled up to gram quantities in satisfactory yields. According to the following experimental facts and related literature reports, a radical pathway was involved in this transformation.

UR - https://www.scopus.com/pages/publications/84926659567

U2 - 10.1039/c5cc00872g

DO - 10.1039/c5cc00872g

M3 - 文章

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AN - SCOPUS:84926659567

SN - 1359-7345

VL - 51

SP - 6839

EP - 6842

JO - Chemical Communications

JF - Chemical Communications

IS - 31

ER -

Metal-free nitro-carbocyclization of 1,6-enynes with tBuONO and TEMPO

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Metal-free nitro-carbocyclization of 1,6-enynes with ^tBuONO and TEMPO