Efficient synthesis of thalifoline and its analogs

Qiang Li; San Qi Zhang; Si Cen Wang; Ming Zhe Zhou

doi:10.1080/00397910802590894

Efficient synthesis of thalifoline and its analogs

Qiang Li
, San Qi Zhang
, Si Cen Wang
, Ming Zhe Zhou

医学部

Xi'an Jiaotong University

科研成果: 期刊稿件 › 文章 › 同行评审

5 引用（Scopus）

摘要

Thalifoline (1) and its analogs were synthesized from methyl 3-hydroxy-4-methoxy benzoate by prenyl etherification, Claisen rearrangement, oxidation, imine formation, reductive amination and intramolecular amidation. The last three steps, imine formation, reductive amination, and intramolecular amidation, were completed in one pot at room temperature.

源语言	英语
页（从-至）	1752-1758
页数	7
期刊	Synthetic Communications
卷	39
期	10
DOI	https://doi.org/10.1080/00397910802590894
出版状态	已出版 - 2009

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10.1080/00397910802590894

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title = "Efficient synthesis of thalifoline and its analogs",

abstract = "Thalifoline (1) and its analogs were synthesized from methyl 3-hydroxy-4-methoxy benzoate by prenyl etherification, Claisen rearrangement, oxidation, imine formation, reductive amination and intramolecular amidation. The last three steps, imine formation, reductive amination, and intramolecular amidation, were completed in one pot at room temperature.",

keywords = "Claisen rearrangement, Intramolecular amidation, Isoquinolinone, One-pot method, Thalifoline",

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AB - Thalifoline (1) and its analogs were synthesized from methyl 3-hydroxy-4-methoxy benzoate by prenyl etherification, Claisen rearrangement, oxidation, imine formation, reductive amination and intramolecular amidation. The last three steps, imine formation, reductive amination, and intramolecular amidation, were completed in one pot at room temperature.

KW - Claisen rearrangement

KW - Intramolecular amidation

KW - Isoquinolinone

KW - One-pot method

KW - Thalifoline

UR - https://www.scopus.com/pages/publications/67650047660

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DO - 10.1080/00397910802590894

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Efficient synthesis of thalifoline and its analogs

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