TY - JOUR
T1 - Effect of reticular non-metal inclusions on impact toughness of WR13 tool and die steels
AU - Long, Haixiao
AU - Cao, Rui
AU - Lin, Tongwei
AU - Huo, Xilong
AU - Deng, Shengwei
AU - Liang, Chen
AU - Nan, Hao
AU - Zhao, Wanlin
AU - Wang, Tiejun
N1 - Publisher Copyright:
© 2026, University of Science and Technology Beijing. All rights reserved.
PY - 2026
Y1 - 2026
N2 - To explore the influence of the continuous inclusion network on the impact performance of WR13 tool and die steels, the WR13 alloy powders were prepared by argon atomization and formed by hot isostatic pressing sintering. Taking the imported low-oxygen-content WR13 alloy powders (mass fraction) and the corresponding ingots as the contrast, the microstructure and mechanical properties of the WR13 alloy powders and the corresponding ingots were carried out by oxygen-nitrogen-hydrogen analyzer, laser particle size analyzer, scanning electron microscope, and pendulum impact tester. The results demonstrate that the formation of the reticular inclusions is closely related to the coupling effect between alloy powder particle size and oxygen content. The reticular inclusions formed by Al₂O₃ particles are observed exclusively in ingots prepared by small-sized and high-oxygen-content alloy powders. These inclusions disrupt the metallurgical bonding between the substrates and induce the stress concentration due to the deformation mismatch with the substrates, serving as the primary initiators of crack formation. Comparative results show that, the ingots without continuous reticular inclusions achieve the impact energy of (17.5± 3.08) J, whereas those containing such inclusions exhibit the reduced impact energy of (7.9± 3.97) J, with significant fluctuations. Fracture images reveal that, the larger the inclusion size and the greater the inclusion quantity in the ingots, the easier it is for the cracks to initiate and propagate, ultimately leading to the decrease in impact performance and poor stability of the ingots.
AB - To explore the influence of the continuous inclusion network on the impact performance of WR13 tool and die steels, the WR13 alloy powders were prepared by argon atomization and formed by hot isostatic pressing sintering. Taking the imported low-oxygen-content WR13 alloy powders (mass fraction) and the corresponding ingots as the contrast, the microstructure and mechanical properties of the WR13 alloy powders and the corresponding ingots were carried out by oxygen-nitrogen-hydrogen analyzer, laser particle size analyzer, scanning electron microscope, and pendulum impact tester. The results demonstrate that the formation of the reticular inclusions is closely related to the coupling effect between alloy powder particle size and oxygen content. The reticular inclusions formed by Al₂O₃ particles are observed exclusively in ingots prepared by small-sized and high-oxygen-content alloy powders. These inclusions disrupt the metallurgical bonding between the substrates and induce the stress concentration due to the deformation mismatch with the substrates, serving as the primary initiators of crack formation. Comparative results show that, the ingots without continuous reticular inclusions achieve the impact energy of (17.5± 3.08) J, whereas those containing such inclusions exhibit the reduced impact energy of (7.9± 3.97) J, with significant fluctuations. Fracture images reveal that, the larger the inclusion size and the greater the inclusion quantity in the ingots, the easier it is for the cracks to initiate and propagate, ultimately leading to the decrease in impact performance and poor stability of the ingots.
KW - hot isostatic pressing
KW - impact toughness
KW - reticular non-metal inclusions
KW - tool and die steels
UR - https://www.scopus.com/pages/publications/105036338074
U2 - 10.19591/j.cnki.cn11-1974/tf.2025030014
DO - 10.19591/j.cnki.cn11-1974/tf.2025030014
M3 - 文章
AN - SCOPUS:105036338074
SN - 1001-3784
VL - 44
SP - 193
EP - 209
JO - Fenmo Yejin Jishu/Powder Metallurgy Technology
JF - Fenmo Yejin Jishu/Powder Metallurgy Technology
IS - 2
ER -