Characterization of power-law constitutive relationship of nickel-based single crystal superalloys under different loading rates by nanoindentation with different types of indenters

This work attempts to explore a method to characterize the effect of loading rate on the power-law constitutive parameters of nickel-based single crystal superalloys (NBSX) by nanoindentation, which avoids the influence of indentation sinking-in or piling-up and indentation size effects. Specifically, combing the reduced modulus obtained from a cylindrical flat punch indentation test with the indentation contact stiffness obtained from two pyramidal indentation tests with different equivalent half cone angles, the actual indentation projected contact area of two pyramidal indenters can be acquired. Based on the actual projected contact area and the intrinsic hardness results calculated by Nix-Gao model, the corrected indentation load-depth curves from two pyramidal indenters are constructed. The elastic modulus can be known from the reduced modulus in advance, and then according to the equivalent half cone angle of the pyramidal indenters and the corrected indentation load-depth curves, the representative strain and stress of two pyramidal indenters are obtained, respectively. The power-law constitutive parameters of NBSX along [0 0 1] orientation under different loading rates are accomplished by inverse analyses of the representative stress and strain of two pyramidal indenters, and verified by the test results of a pyramidal indenter with another equivalent half cone angle. Results demonstrate the effectiveness of the explored method.