Application of ultrasonic wave to clean the surface of the TiO                         2                          nanotubes prepared by the electrochemical anodization

Hao Xu; Qian Zhang; Chunli Zheng; Wei Yan; Wei Chu

doi:10.1016/j.apsusc.2011.04.135

Application of ultrasonic wave to clean the surface of the TiO ₂ nanotubes prepared by the electrochemical anodization

Hao Xu
, Qian Zhang
, Chunli Zheng
, Wei Yan
, Wei Chu

能源与动力工程学院

Hong Kong Polytechnic University
Xi'an Jiaotong University

科研成果: 期刊稿件 › 文章 › 同行评审

52 引用（Scopus）

摘要

In this study, the TiO ₂ nanotubes were fabricated by electrochemical anodization in a NH ₄ F/Na ₂ SO ₄ /PEG400/H ₂ O electrolyte system. Ultrasonic wave (80 W, 40 kHz) was used to clean the surface of TiO ₂ nanotube arrays in the medium of water after the completion of the anodization. Surface morphology (FESEM) and X-ray diffraction spectrum of the nanotubes treated by sonication at 0 min, 9 min, 40 min and 60 min were compared. The experimental results showed that the precipitate on the surface of the nanotube arrays could be removed by the ultrasonic wave. The treating time had an influence on the precipitate removal and 9 min (corresponding to 12 Wh) is the suitable time for surface cleaning of the TiO ₂ nanotubes on this experimental condition.

源语言	英语
页（从-至）	8478-8480
页数	3
期刊	Applied Surface Science
卷	257
期	20
DOI	https://doi.org/10.1016/j.apsusc.2011.04.135
出版状态	已出版 - 1 8月 2011

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10.1016/j.apsusc.2011.04.135

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@article{8ef6b0edf8a240d9b2906fc6d451a32c,

title = " Application of ultrasonic wave to clean the surface of the TiO 2 nanotubes prepared by the electrochemical anodization ",

abstract = " In this study, the TiO 2 nanotubes were fabricated by electrochemical anodization in a NH 4 F/Na 2 SO 4 /PEG400/H 2 O electrolyte system. Ultrasonic wave (80 W, 40 kHz) was used to clean the surface of TiO 2 nanotube arrays in the medium of water after the completion of the anodization. Surface morphology (FESEM) and X-ray diffraction spectrum of the nanotubes treated by sonication at 0 min, 9 min, 40 min and 60 min were compared. The experimental results showed that the precipitate on the surface of the nanotube arrays could be removed by the ultrasonic wave. The treating time had an influence on the precipitate removal and 9 min (corresponding to 12 Wh) is the suitable time for surface cleaning of the TiO 2 nanotubes on this experimental condition.",

keywords = "Electrochemical anodization, Microstructure, Surfaces, Ultrasonic wave",

author = "Hao Xu and Qian Zhang and Chunli Zheng and Wei Yan and Wei Chu",

year = "2011",

month = aug,

day = "1",

doi = "10.1016/j.apsusc.2011.04.135",

language = "英语",

volume = "257",

pages = "8478--8480",

journal = "Applied Surface Science",

issn = "0169-4332",

publisher = "Elsevier B.V.",

number = "20",

}

Xu, H, Zhang, Q, Zheng, C , Yan, W & Chu, W 2011, ' Application of ultrasonic wave to clean the surface of the TiO ₂ nanotubes prepared by the electrochemical anodization ', Applied Surface Science, 卷 257, 号码 20, 页码 8478-8480. https://doi.org/10.1016/j.apsusc.2011.04.135

Application of ultrasonic wave to clean the surface of the TiO ₂ nanotubes prepared by the electrochemical anodization . / Xu, Hao; Zhang, Qian; Zheng, Chunli 等.
在: Applied Surface Science, 卷 257, 号码 20, 01.08.2011, 页码 8478-8480.

科研成果: 期刊稿件 › 文章 › 同行评审

TY - JOUR

T1 - Application of ultrasonic wave to clean the surface of the TiO 2 nanotubes prepared by the electrochemical anodization

AU - Xu, Hao

AU - Zhang, Qian

AU - Zheng, Chunli

AU - Yan, Wei

AU - Chu, Wei

PY - 2011/8/1

Y1 - 2011/8/1

N2 - In this study, the TiO 2 nanotubes were fabricated by electrochemical anodization in a NH 4 F/Na 2 SO 4 /PEG400/H 2 O electrolyte system. Ultrasonic wave (80 W, 40 kHz) was used to clean the surface of TiO 2 nanotube arrays in the medium of water after the completion of the anodization. Surface morphology (FESEM) and X-ray diffraction spectrum of the nanotubes treated by sonication at 0 min, 9 min, 40 min and 60 min were compared. The experimental results showed that the precipitate on the surface of the nanotube arrays could be removed by the ultrasonic wave. The treating time had an influence on the precipitate removal and 9 min (corresponding to 12 Wh) is the suitable time for surface cleaning of the TiO 2 nanotubes on this experimental condition.

AB - In this study, the TiO 2 nanotubes were fabricated by electrochemical anodization in a NH 4 F/Na 2 SO 4 /PEG400/H 2 O electrolyte system. Ultrasonic wave (80 W, 40 kHz) was used to clean the surface of TiO 2 nanotube arrays in the medium of water after the completion of the anodization. Surface morphology (FESEM) and X-ray diffraction spectrum of the nanotubes treated by sonication at 0 min, 9 min, 40 min and 60 min were compared. The experimental results showed that the precipitate on the surface of the nanotube arrays could be removed by the ultrasonic wave. The treating time had an influence on the precipitate removal and 9 min (corresponding to 12 Wh) is the suitable time for surface cleaning of the TiO 2 nanotubes on this experimental condition.

KW - Electrochemical anodization

KW - Microstructure

KW - Surfaces

KW - Ultrasonic wave

UR - https://www.scopus.com/pages/publications/79959357684

U2 - 10.1016/j.apsusc.2011.04.135

DO - 10.1016/j.apsusc.2011.04.135

M3 - 文章

AN - SCOPUS:79959357684

SN - 0169-4332

VL - 257

SP - 8478

EP - 8480

JO - Applied Surface Science

JF - Applied Surface Science

IS - 20

ER -

Application of ultrasonic wave to clean the surface of the TiO 2 nanotubes prepared by the electrochemical anodization

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Application of ultrasonic wave to clean the surface of the TiO ₂ nanotubes prepared by the electrochemical anodization