3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3- thiazole-5-carboxylate ethyl ester

Ge Meng; Mei Wang; Ya Nan Cheng; Kai Chen; Jing Tong; Jie He Zhang

doi:10.3390/M919

3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3- thiazole-5-carboxylate ethyl ester

Ge Meng
, Mei Wang
, Ya Nan Cheng
, Kai Chen
, Jing Tong
, Jie He Zhang

材料科学与工程学院

Xi'an Jiaotong University

科研成果: 期刊稿件 › 评论/辩论

摘要

An efficient procedure to obtain the new compound 1a from ethyl acetoacetate (2a), NBS and N,N0-diethylthiourea (4a) was reported. In comparison with the traditional method to synthesize its analogues, this efficient, catalyst-free, and one-pot synthetic method is facile. The work-up procedure is easy and gives the pure target compound under milder reaction conditions in a relatively high yield of 75%.

源语言	英语
文章编号	M919
期刊	MolBank
卷	2016
期	4
DOI	https://doi.org/10.3390/M919
出版状态	已出版 - 1 12月 2016

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@article{8956c865bfb146a4951d251b602645e2,

title = "3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3- thiazole-5-carboxylate ethyl ester",

abstract = "An efficient procedure to obtain the new compound 1a from ethyl acetoacetate (2a), NBS and N,N0-diethylthiourea (4a) was reported. In comparison with the traditional method to synthesize its analogues, this efficient, catalyst-free, and one-pot synthetic method is facile. The work-up procedure is easy and gives the pure target compound under milder reaction conditions in a relatively high yield of 75\%.",

keywords = "2,3-dihydro-1,3-thiazole, N,N′-diethylthiourea, One-pot synthesis",

author = "Ge Meng and Mei Wang and Cheng, \{Ya Nan\} and Kai Chen and Jing Tong and Zhang, \{Jie He\}",

note = "Publisher Copyright: {\textcopyright} 2016 by the author; licensee MDPI, Basel, Switzerland.",

year = "2016",

month = dec,

day = "1",

doi = "10.3390/M919",

language = "英语",

volume = "2016",

journal = "MolBank",

issn = "1422-8599",

publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",

number = "4",

}

TY - JOUR

T1 - 3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3- thiazole-5-carboxylate ethyl ester

AU - Meng, Ge

AU - Wang, Mei

AU - Cheng, Ya Nan

AU - Chen, Kai

AU - Tong, Jing

AU - Zhang, Jie He

PY - 2016/12/1

Y1 - 2016/12/1

N2 - An efficient procedure to obtain the new compound 1a from ethyl acetoacetate (2a), NBS and N,N0-diethylthiourea (4a) was reported. In comparison with the traditional method to synthesize its analogues, this efficient, catalyst-free, and one-pot synthetic method is facile. The work-up procedure is easy and gives the pure target compound under milder reaction conditions in a relatively high yield of 75%.

AB - An efficient procedure to obtain the new compound 1a from ethyl acetoacetate (2a), NBS and N,N0-diethylthiourea (4a) was reported. In comparison with the traditional method to synthesize its analogues, this efficient, catalyst-free, and one-pot synthetic method is facile. The work-up procedure is easy and gives the pure target compound under milder reaction conditions in a relatively high yield of 75%.

KW - 2,3-dihydro-1,3-thiazole

KW - N,N′-diethylthiourea

KW - One-pot synthesis

UR - https://www.scopus.com/pages/publications/85003683083

U2 - 10.3390/M919

DO - 10.3390/M919

M3 - 评论/辩论

AN - SCOPUS:85003683083

SN - 1422-8599

VL - 2016

JO - MolBank

JF - MolBank

IS - 4

M1 - M919

ER -

3-Ethyl-2-(ethylimino)-4-methyl-2,3-dihydro-1,3- thiazole-5-carboxylate ethyl ester

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