Visible-light-driven palladium-catalyzed Dowd-Beckwith ring expansion/C-C bond formation cascade

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Abstract

A visible-light-induced palladium-catalyzed Dowd-Beckwith ring expansion/C-C bond formation cascade is described. A range of six to nine-membered β-alkenylated cyclic ketones possessing a quaternary carbon center were accessed under mild conditions. Besides styrenes, the electron-rich alkenes such as silyl enol ethers and enamides were also compatible, providing the desired β-alkylated cyclic ketones in moderate to good yields.

Original languageEnglish
Pages (from-to)1791-1795
Number of pages5
JournalChemical Science
Volume12
Issue number5
DOIs
StatePublished - 7 Feb 2021

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