Synthesis of nanocrystalline titania films by micro-arc oxidation

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Abstract

Nanocrystalline titania films were synthesized by micro-arc oxidation of titanium substrates in an electrolytic solution using a pulsed power supply. X-ray diffraction (XRD) indicated that the deposited films consisted of a high crystalline anatase phase. Field emission scanning electron microscopy (FESEM) showed that the films were macro-porous with 1-2 μm pores and the matrix was composed of 10-20 nm grains. The adhesion-tension test showed that the films had an adhesive strength of 20 ± 2MPa. Such firmly adhesive, porous and nanocrystalline anatase films are expected to have significant applications as orthopaedic/dental implants and catalysts.

Original languageEnglish
Pages (from-to)744-747
Number of pages4
JournalMaterials Letters
Volume56
Issue number5
DOIs
StatePublished - Nov 2002

Keywords

  • Adhesive strength
  • Micro-arc oxidation
  • Nanocrystalline
  • Titania film

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