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Synthesis and characterization of polyimide/silica nanocomposite films

  • M. Y. Zhang
  • , S. J. Zeng
  • , T. Q. Dong
  • , Y. Fan
  • , Q. Q. Lei
  • Harbin University of Science and Technology

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

2 Scopus citations

Abstract

In the paper, a kind of polyimide nanocomposite films was made by synthesizing polyimide/silica nano-particle matrix resin through the hydrolysis and poly-condensation of varies ratio of tetraethoxysilane (TEOS) and dimethyldiethoxysilane (DMES) in the solution of polyamic acid (PAA) solution dissolved in N, N-dimethylacetamide (DMAc), followed by rotating it on glass substrates and heating at high temperature. The 3-aminopropyltriethoxysilane (APrTEOS), which serves as a coupling agent, was chosen to enhance the compatibility between the polyimide (PI) and the silica (SiO2). The chemical structure of the films was characterized by FT-IR. The results of TGA proved that the thermal stability can be improved by well dispersion of inorganic components not more than 16wt%.

Original languageEnglish
Title of host publication2007 International Conference on Solid Dielectrics, ICSD
Pages357-359
Number of pages3
DOIs
StatePublished - 2007
Externally publishedYes
Event2007 International Conference on Solid Dielectrics, ICSD - Winchester, United Kingdom
Duration: 8 Jul 200713 Jul 2007

Publication series

Name2007 International Conference on Solid Dielectrics, ICSD

Conference

Conference2007 International Conference on Solid Dielectrics, ICSD
Country/TerritoryUnited Kingdom
CityWinchester
Period8/07/0713/07/07

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