Real-time neutron scattering study of transient phases in polymer crystallization

Xiangbing Zeng; Goran Ungar; Stephen J. Spells; Stephen M. King

doi:10.1021/ma0510486

Real-time neutron scattering study of transient phases in polymer crystallization

Xiangbing Zeng
, Goran Ungar
, Stephen J. Spells
, Stephen M. King

University of Sheffield
Sheffield Hallam University
Rutherford Appleton Laboratory

Research output: Contribution to journal › Article › peer-review

27 Scopus citations

Abstract

The mapping of the transient phases in polymer crystallization were studied using small-angle neutron and X-ray scattering (SANS and SAXS). Polymer crystallization is a highly nonequilibrium process and is often accompanied by the appearance of transient forms and solid-state transformations. SAXS data with a reasonable signal-to-noise ratio can be collected in subsecond frames using synchrotron radiation sources. It was observed that SANS data of similar signal-to-noise ratio take hours to collect and this makes real-time SAXS suitable for studies of the crystallization process in polymers and other materials.

Original language	English
Pages (from-to)	7201-7204
Number of pages	4
Journal	Macromolecules
Volume	38
Issue number	17
DOIs	https://doi.org/10.1021/ma0510486
State	Published - 23 Aug 2005
Externally published	Yes

Access to Document

10.1021/ma0510486

Cite this

@article{8ffbc1e7745c4ac3849f5b66f1026436,

title = "Real-time neutron scattering study of transient phases in polymer crystallization",

abstract = "The mapping of the transient phases in polymer crystallization were studied using small-angle neutron and X-ray scattering (SANS and SAXS). Polymer crystallization is a highly nonequilibrium process and is often accompanied by the appearance of transient forms and solid-state transformations. SAXS data with a reasonable signal-to-noise ratio can be collected in subsecond frames using synchrotron radiation sources. It was observed that SANS data of similar signal-to-noise ratio take hours to collect and this makes real-time SAXS suitable for studies of the crystallization process in polymers and other materials.",

author = "Xiangbing Zeng and Goran Ungar and Spells, \{Stephen J.\} and King, \{Stephen M.\}",

year = "2005",

month = aug,

day = "23",

doi = "10.1021/ma0510486",

language = "英语",

volume = "38",

pages = "7201--7204",

journal = "Macromolecules",

issn = "0024-9297",

publisher = "American Chemical Society",

number = "17",

}

TY - JOUR

T1 - Real-time neutron scattering study of transient phases in polymer crystallization

AU - Zeng, Xiangbing

AU - Ungar, Goran

AU - Spells, Stephen J.

AU - King, Stephen M.

PY - 2005/8/23

Y1 - 2005/8/23

N2 - The mapping of the transient phases in polymer crystallization were studied using small-angle neutron and X-ray scattering (SANS and SAXS). Polymer crystallization is a highly nonequilibrium process and is often accompanied by the appearance of transient forms and solid-state transformations. SAXS data with a reasonable signal-to-noise ratio can be collected in subsecond frames using synchrotron radiation sources. It was observed that SANS data of similar signal-to-noise ratio take hours to collect and this makes real-time SAXS suitable for studies of the crystallization process in polymers and other materials.

AB - The mapping of the transient phases in polymer crystallization were studied using small-angle neutron and X-ray scattering (SANS and SAXS). Polymer crystallization is a highly nonequilibrium process and is often accompanied by the appearance of transient forms and solid-state transformations. SAXS data with a reasonable signal-to-noise ratio can be collected in subsecond frames using synchrotron radiation sources. It was observed that SANS data of similar signal-to-noise ratio take hours to collect and this makes real-time SAXS suitable for studies of the crystallization process in polymers and other materials.

UR - https://www.scopus.com/pages/publications/24944537156

U2 - 10.1021/ma0510486

DO - 10.1021/ma0510486

M3 - 文章

AN - SCOPUS:24944537156

SN - 0024-9297

VL - 38

SP - 7201

EP - 7204

JO - Macromolecules

JF - Macromolecules

IS - 17

ER -

Real-time neutron scattering study of transient phases in polymer crystallization

Abstract

Access to Document

Other files and links

Fingerprint

Cite this