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Microstructure and mechanical properties of nanocrystalline tungsten thin films

  • Xi'an Jiaotong University

Research output: Contribution to journalArticlepeer-review

72 Scopus citations

Abstract

Tungsten (W) thin films were prepared by magnetron sputtering onto Si (100) substrates. Their microstructures were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). The hardness and modulus were evaluated by nanoindentation. It is found that a 30 nm Cr sticking layer induces structure changes of deposited W film from β-W to α-W structure. In addition, remarkable hardness enhancement both for the deposited and annealed W films, were compared with that of bulk coarse-grained W, although their nanoindentation modulus is very close to that of corresponding bulk W. The intrinsic reasons that lead to structure changes and super hardness are discussed.

Original languageEnglish
Pages (from-to)87-92
Number of pages6
JournalJournal of Materials Science and Technology
Volume26
Issue number1
DOIs
StatePublished - Jan 2010

Keywords

  • Hardness
  • Microstructure
  • Modulus
  • Nanoindentation
  • Tungsten film

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