Flowerlike cubic β-In2S3 microspheres: Synthesis and characterization

Lijun Liu; Weidong Xiang; Jiasong Zhong; Xinyu Yang; Xiaojuan Liang; Haitao Liu; Wen Cai

doi:10.1016/j.jallcom.2009.12.089

Flowerlike cubic β-In₂S₃ microspheres: Synthesis and characterization

Lijun Liu
, Weidong Xiang
, Jiasong Zhong
, Xinyu Yang
, Xiaojuan Liang
, Haitao Liu
, Wen Cai

Wenzhou University
Tongji University

Research output: Contribution to journal › Article › peer-review

37 Scopus citations

Abstract

Flowerlike cubic beta-indium (III) sulfide (β-In₂S₃) microspheres were synthesized via a one-step solvothermal route, in which thiosalicylic acid (TSA) and carbon disulfide (CS₂) were used as the double sulfur sources. The phase structure, morphology and composition of the products were characterized by means of X-ray powder diffraction (XRD), field-emission scanning microscopy (FESEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED). The thermal behavior and the optical properties were investigated by thermogravimetric (TG) measurements and UV-vis spectrophotometer, respectively. Furthermore, the role of TSA was studied by the Fourier transform infrared spectroscopy (FTIR), and a possible mechanism for the growth of the flowerlike cubic β-In₂S₃ microspheres was proposed. Crown

Original language	English
Pages (from-to)	309-313
Number of pages	5
Journal	Journal of Alloys and Compounds
Volume	493
Issue number	1-2
DOIs	https://doi.org/10.1016/j.jallcom.2009.12.089
State	Published - 18 Mar 2010
Externally published	Yes

Keywords

Chemical synthesis
Inorganic material
Microstructure
Optical properties
SEM
TEM
Thermal analysis
X-ray diffraction

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10.1016/j.jallcom.2009.12.089

Cite this

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title = "Flowerlike cubic β-In2S3 microspheres: Synthesis and characterization",

abstract = "Flowerlike cubic beta-indium (III) sulfide (β-In2S3) microspheres were synthesized via a one-step solvothermal route, in which thiosalicylic acid (TSA) and carbon disulfide (CS2) were used as the double sulfur sources. The phase structure, morphology and composition of the products were characterized by means of X-ray powder diffraction (XRD), field-emission scanning microscopy (FESEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED). The thermal behavior and the optical properties were investigated by thermogravimetric (TG) measurements and UV-vis spectrophotometer, respectively. Furthermore, the role of TSA was studied by the Fourier transform infrared spectroscopy (FTIR), and a possible mechanism for the growth of the flowerlike cubic β-In2S3 microspheres was proposed. Crown",

keywords = "Chemical synthesis, Inorganic material, Microstructure, Optical properties, SEM, TEM, Thermal analysis, X-ray diffraction",

author = "Lijun Liu and Weidong Xiang and Jiasong Zhong and Xinyu Yang and Xiaojuan Liang and Haitao Liu and Wen Cai",

year = "2010",

month = mar,

day = "18",

doi = "10.1016/j.jallcom.2009.12.089",

language = "英语",

volume = "493",

pages = "309--313",

journal = "Journal of Alloys and Compounds",

issn = "0925-8388",

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TY - JOUR

T1 - Flowerlike cubic β-In2S3 microspheres

T2 - Synthesis and characterization

AU - Liu, Lijun

AU - Xiang, Weidong

AU - Zhong, Jiasong

AU - Yang, Xinyu

AU - Liang, Xiaojuan

AU - Liu, Haitao

AU - Cai, Wen

PY - 2010/3/18

Y1 - 2010/3/18

N2 - Flowerlike cubic beta-indium (III) sulfide (β-In2S3) microspheres were synthesized via a one-step solvothermal route, in which thiosalicylic acid (TSA) and carbon disulfide (CS2) were used as the double sulfur sources. The phase structure, morphology and composition of the products were characterized by means of X-ray powder diffraction (XRD), field-emission scanning microscopy (FESEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED). The thermal behavior and the optical properties were investigated by thermogravimetric (TG) measurements and UV-vis spectrophotometer, respectively. Furthermore, the role of TSA was studied by the Fourier transform infrared spectroscopy (FTIR), and a possible mechanism for the growth of the flowerlike cubic β-In2S3 microspheres was proposed. Crown

AB - Flowerlike cubic beta-indium (III) sulfide (β-In2S3) microspheres were synthesized via a one-step solvothermal route, in which thiosalicylic acid (TSA) and carbon disulfide (CS2) were used as the double sulfur sources. The phase structure, morphology and composition of the products were characterized by means of X-ray powder diffraction (XRD), field-emission scanning microscopy (FESEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED). The thermal behavior and the optical properties were investigated by thermogravimetric (TG) measurements and UV-vis spectrophotometer, respectively. Furthermore, the role of TSA was studied by the Fourier transform infrared spectroscopy (FTIR), and a possible mechanism for the growth of the flowerlike cubic β-In2S3 microspheres was proposed. Crown

KW - Chemical synthesis

KW - Inorganic material

KW - Microstructure

KW - Optical properties

KW - SEM

KW - TEM

KW - Thermal analysis

KW - X-ray diffraction

UR - https://www.scopus.com/pages/publications/77249153803

U2 - 10.1016/j.jallcom.2009.12.089

DO - 10.1016/j.jallcom.2009.12.089

M3 - 文章

AN - SCOPUS:77249153803

SN - 0925-8388

VL - 493

SP - 309

EP - 313

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

IS - 1-2

ER -

Flowerlike cubic β-In₂S₃ microspheres: Synthesis and characterization

Abstract

Keywords

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