Characterization of microstructure of nano-TiO 2 coating deposited by vacuum cold spraying

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Abstract

Control of the microstructure of TiO 2 coatings through preparation methods significantly influences the coating performance. In this study, a vacuum cold-spray process, as a new coating technology, is used to deposit nanocrystalline TiO 2, coatings on conducting glass and stainless steel substrates. TiO 2, deposits were formed using two types of nanocrystalline TiO 2 powders with mean particle diameters of 200 and 25 nm. Coating microstructures were characterized by scanning electron microscopy and x-ray diffraction analysis. Results demonstrate that a thick nanocrystalline TiO 2 coating can be deposited by the vacuum cold-spray process. The coating was found to consist of particles stacked as agglomerates that build up to several hundred nanometers. The coating also presents a mesoporous microstructure that could be effective in such applications as photocatalytic degradation and dye-sensitized solar cells.

Original languageEnglish
Pages (from-to)513-517
Number of pages5
JournalJournal of Thermal Spray Technology
Volume15
Issue number4
DOIs
StatePublished - Dec 2006

Keywords

  • Ceramic coating
  • Mesoporous structure
  • Nanocrystalline material
  • TiO
  • Vacuum cold spray

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