Annealing effect on the intermetallic compound formation of cold sprayed Fe/Al

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Abstract

A Fe/Al composite coating was prepared by cold spraying using an iron-aluminium powder mixture with a Fe/Al atomic ratio of 1:1. The effect of annealing temperature on the intermetallic compound formation in the cold-sprayed Fe/Al coating was investigated. The as-sprayed and annealed coatings were characterized by x-ray diffraction (XRD), and scanning electron microscopy (SEM) equipped with energy dispersive spectroscopy. Results showed that intensive particle deformation on impact promoted the Fe 2Al 5 intermetallic compound formation at a low annealing temperature of 450°C and this intermetallic layer firstly appeared along some intimate contact regions at the aluminium-iron boundaries. The amount of the Fe2Al5 intermetallic compound increased and no other intermetallic compound phases appeared when the annealing temperature was raised from 450 to 600°C. Some cracks developed in the Fe2Al5 intermetallic layer when the coating was annealed at 600°C and the possible causes leading to evolution of cracks are discussed.

Original languageEnglish
Pages (from-to)571-577
Number of pages7
JournalJournal of Thermal Spray Technology
Volume21
Issue number3-4
DOIs
StatePublished - Jun 2012

Keywords

  • Annealing
  • Coating
  • Cold spray
  • Fe/Al composite
  • Intermetallics
  • Microstructure

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